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the alumina, two zones that fluoresce blue can be spotted by
illumination with a black light. The faster-moving zone contains LSD,
while the slower-moving zone is iso-LSD.
When the zone containing LSD reaches the spigot of the burette, it
should be collected in a separate flask. About 3000 ml of the 3-1
benzene-chloroform is required to get the LSD moved down the
chromatography column, and finally eluted.
The iso-LSD is then flushed from the column by switching the
solvent being fed into the top of the column to chloroform. This
material is collected in a separate flask, and the solvent removed
under a vacuum. The residue is iso-LSD, and should be stored in the
freezer until conversion to LSD is undertaken.
Directions for this are also given in this chapter.
For the fraction containing the LSD, conversion to LSD tartrate must be done to make it water soluble, improve its keeping characteristics, and to allow crystallization. Tartaric acid has the ability to react with two molecules of LSD. Use, then, of a 50% excess of tartaric acid dictates the use of about 1 gram of tartaric acid to 3 grams of LSD. The three grams of LSD would be expected from a well-done batch out of a total 3.5 LSD/iso-LSD mix. The crystalline tartrate is made by dissolving one gram of tartaric acid in a few mis of methanol, and adding this acid solution to the benzene-chloroform elute from the chromatography column. Evaporation of the solvent to a low volume under a vacuum gives crystalline LSD tartrate. Crystals are often difficult to obtain. Instead, an oil may result due to the presence of impurities. This is not cause for alarm; the oil is still likely 90%+ pure. It should be bottled up in dark glass, preferably under a nitrogen atmosphere, and kept in a freezer until moved. If chromatography reveals that one's chosen cooking method produces little of the iso products, then the production of the tartrate salt and crystallization is simplified. The residue obtained at the end Practical LSD Manufacture 32 of the batch is dissolved in a minimum amount of methanol. To this is then added tartaric acid. The same amount is added as above: one gram tartaric acid to three grams LSD. Next, ether is slowly added with vigorous stirring until a precipitate begins to form. The stoppered flask is then
Super Strength Kratom Whole Leaf (Mitragyna Speciosa)put in the freezer overnight to complete the precipitation.
After filtering or centrifuging to isolate the product, it is transferred to a dark bottle, preferably under nitrogen, and kept in the freezer until moved. LSD from (so-LSD Two variations on this procedure will be presented here. The first is the method of Smith and Timmis from The Journal of the Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is found in US patent 2,736,728.
Both use the action of a strong hydroxide solution to convert iso material into a mixture that contains active and iso material. At equilibrium, the mixture contains about 2/3 caapi) YELLOW Vine (Banisteriopsis Hawaiian Seeds Seeds Seeds Hawaiian Bali Lily Color Blend (Nyphaea sp) nt a bunch of thallium around the house about like you want to be kicked in the teeth with a heavy pair of boots. A further bad aspect of this method is its high cost. 100 grams sell for $150, and the high molecular weight of the compound means that a lot of it has to be used to get a moderate amount of product. One pound of thallium(ni) nitrate is required for a 1-molar batch. This method can be found in Tetrahedron Letters No. 60, pages 5275-80 (1970). To produce a one mole batch, dissolve one mole of propenylbenzene in some methanol, and put it into a one-gallon glass jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate trihydrate in methanol. Then pour the thallium solution into the jug with the propenylbenzene, and stir at room temperature for 5 minutes. The thallium(I) nitrate formed by the reaction comes out of solution. It is removed by filtration. The propenylbenzene has at this point been converted to a ketal. This is hydrolyzed to the phenylacetone by shaking the filtrate with about 2000 ml of 1 molar sulfuric acid solution in water for about 5 minutes. The phenylacetone is then extracted out with a couple of portions of tolulene. This extract is then washed with 5% NaOH solution, then distilled or purified by conversion to the bisulfite addition product. 12 Studies On The Production OfTMA-2 93 Production of TMA-2, MDA, etc. from the Corresponding Phenylacetone There are three good methods for converting the phenylacetone to the psychedelic amphetamine. Choice number one is to use reductive amination with a hydrogenation bomb with Raney nickel, ammonia and alcohol solvent. See Journal of the American Chemical Society, Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from 1954, column 2097. This gives a yield of about 80% if plenty of Raney nickel is used. The preferred conditions for use with MDA is a temperature of 80 C, and a hydrogen pressure of 50 atmospheres. The drawback to this method is the need for a shaker device for the bomb, and also a heater. The use of platinum as the catalyst in the bomb works great when making MDMA, but gives lousy results when making MDA. There may be a way around this, however, for serious experimenters. It has been found in experiments with phenylacetone that a mixture of ammonia and ammonium chloride produces good yields of amphetamine (50%) when used in a bomb with platinum catalyst. Methylenedioxyphenylacetone is quite likely to behave similarly, along with other phenylacetones. To use this variation, the following materials are placed in the 1.5 liter champagne bottle hydrogenation device described in Chapter 11 of Secrets of Methamphetamine Manufacture, Third Edition: .5 gram platinum in 20 ml distilled water. If this platinum is in the form of PtO2 instead of reduced platinum metal catalyst obtained with borohydride, the experimenter must now reduce the platinum by pressurizing the bottle with hydrogen and stirring fo Hawaiian Seeds Seeds Seeds Hawaiian Contact
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