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erature reading lesson to those who have made these claims. See Proceedings of the Royal Society of London, Series B, Volume 155, pages 26 to 54 (1961). Also see US Patent 3,219,545. You will note while reading these articles detailing how to get lysergic amide production in a culture medium that these guys had to scour the globe to find that rare strain of claviceps fungus that will cooperate in this manner. The vast majority of claviceps fungi just will not produce these alkaloids while being cultured. See the following articles to convince yourself of just how futile it is to collect a wild strain of claviceps and try to get it to produce lysergic acid amides in culture: Ann. Rep. Takeda Res. Lab Volume 10, page 73 (1951); and Farmco, Volume 1, page 1 (1946); also Arch. Pharm. Berl. Volume 273, page 348 (1935); also American Journal of Practical LSD Manufacture Botany, Volume 18, page 50 (1931); also Journal of the American Pharmacy Association Volume 40, page 434 (1951); also US patent 2,809,920; also Canadian Journal of Microbiology, Volume 3, page 55 (1957), and Volume 4, page 611 (1958) and Volume 6, page 355 (1960); also Journal of the American Pharmacy Society Volume 44, page 736 (1955). With this matter disposed of, it is time to move on to what actually are viable sources of lysergic acid amides for the production of LSD. This is the farming end of the acid business. It is only through raising ergot-infested rye, or growing morning glories and Hawaiian baby woodrose that the required feedstocks of lysergic compounds can be obtained without making a target of oneself. I have for years seen ads in High Times offering morning glory seeds and Hawaiian baby woodrose seeds for sale, but these are offered in small amounts at high prices. I would bet my bottom dollar that these outfits, if they are not front operations, will at least report to the heat any large orders they get. To avoid detection, the aspiring LSD manufacturer must be ready to get his hands dirty, and spend some time as a farmer. The most difficult farming choice, and as luck would have it, the one that gives the purest acid, is to grow a patch of ergot-infested rye. The reason why ergot is superior to growing morning glory seeds or woodrose seeds is that these seeds have a considerable amount of another type of alkaloid in them besides the ones that yield lysergic acid. These other alkaloids are of the clavine type, meaning that they have the lysergic-acid skeleton, but lack the carboxyl grouping. In its place will be a methyl grouping, an alcohol grouping, a methyl alcohol grouping or combinations of the above. These clavine alkaloids will likely be carried all the way through into the product, producing both the GIGO situation during the synthetic operations and a contaminated product when finished. I will present my ideas on how to remove them, but they are best avoided in the first place. Ergot is the name given to a dark brow “CHACRUNA” Dried Whole Leaf (Psycotria viridis) Red Caapi) Ayahuasca Ayahuasca Red Intoxicating Mint (Lagochilus inebrians) wnward through the alumina, two zones that fluoresce blue can be spotted by illumination with a black light. The faster-moving zone contains LSD, while the slower-moving zone is iso-LSD. When the zone containing LSD reaches the spigot of the burette, it should be collected in a separate flask. About 3000 ml of the 3-1 benzene-chloroform is required to get the LSD moved down the chromatography column, and finally eluted. The iso-LSD is then flushed from the column by switching the solvent being fed into the top of the column to chloroform. This material is collected in a separate flask, and the solvent removed under a vacuum. The residue is iso-LSD, and should be stored in the freezer until conversion to LSD is undertaken. Directions for this are also given in this chapter. For the fraction containing the LSD, conversion to LSD tartrate must be done to make it water soluble, improve its keeping characteristics, and to allow crystallization. Tartaric acid has the ability to react with two molecules of LSD. Use, then, of a 50% excess of tartaric acid dictates the use of about 1 gram of tartaric acid to 3 grams of LSD. The three grams of LSD would be expected from a well-done batch out of a total 3.5 LSD/iso-LSD mix. The crystalline tartrate is made by dissolving one gram of tartaric acid in a few mis of methanol, and adding this acid solution to the benzene-chloroform elute from the chromatography column. Evaporation of the solvent to a low volume under a vacuum gives crystalline LSD tartrate. Crystals are often difficult to obtain. Instead, an oil may result due to the presence of impurities. This is not cause for alarm; the oil is still likely 90%+ pure. It should be bottled up in dark glass, preferably under a nitrogen atmosphere, and kept in a freezer until moved. If chromatography reveals that one's chosen cooking method produces little of the iso products, then the production of the tartrate salt and crystallization is simplified. The residue obtained at the end Practical LSD Manufacture 32 of the batch is dissolved in a minimum amount of methanol. To this is then added tartaric acid. The same amount is added as above: one gram tartaric acid to three grams LSD. Next, ether is slowly added with vigorous stirring until a precipitate begins to form. The stoppered flask is then put in the freezer overnight to complete the precipitation. After filtering or centrifuging to isolate the product, it is transferred to a dark bottle, preferably under nitrogen, and kept in the freezer until moved. LSD from (so-LSD Two variations on this procedure will be presented here. The first is the method of Smith and Timmis from The Journal of the Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is found in US patent 2,736,728. Both use the action of a strong hydroxide solution to convert iso material into a mixture that contains active and iso material. At equilibrium, the mixture contains about 2/3 Hawaiian Baby Woodrose Seeds Red Caapi) Ayahuasca Ayahuasca Red Ayahuasca BLACK (Negra) Vine(Banisteriopsis caapi)VERY POWERFUL Normally ONLY used by Shaman!!
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